超高效液相色谱-串联质谱法测定土壤中烷基酚  

Determination of Alkylphenol in Soil by UPLC-MS/MS

作　　者：王静[1] 潘荷芳[1] 刘铮铮[1] 刘劲松[1] 

机构地区：[1]浙江省环境监测中心,浙江杭州310012

出　　处：《分析测试学报》2007年第z1期210-212,共3页Journal of Instrumental Analysis

摘　　要：A quick and sensitive analytical method for alkylphenols in soil was determined using accelerate solvent extraction and UPLC-MS/MS.It was determined that,analysis of one sample needed only 6 min.Recoveries of 4-tert-octylphenol,4-nonylphenol,4-octylphenol were 82.8%-104%,79.3%-98.4%,92.9%-109%,respectively,at the same time,the detection limit and area RSD were 0.001-0.005 mg/kg,2.0%-3.4%.A quick and sensitive analytical method for alkylphenols in soil was determined using accelerate solvent extraction and UPLC-MS/MS.It was determined that,analysis of one sample needed only 6 min.Recoveries of 4-tert-octylphenol,4-nonylphenol,4-octylphenol were 82.8%-104%,79.3%-98.4%,92.9%-109%,respectively,at the same time,the detection limit and area RSD were 0.001-0.005 mg/kg,2.0%-3.4%.

关 键 词：Soil alkylphenol ANALYSIS UPLC-MS/MS 

分 类 号：O657-55[理学—分析化学]