显微、紫外光谱方法检测羚羊角与山羊角、羚羊角胶囊的真伪和掺骨塞及钙含量  

Methods of the Microscopical identificaton and the uitra-violt spectra to detecet the true and the false of cornu saigae tataricae(CST) and cornu capra hircus(CCH) and cornu saigae tataricae capsules(CSTC)and of the bone adulterant and of the calcium conte

作　　者：朱照祥 茅云霞[2] 

机构地区：[1]浙江省台州市药品检验所,浙江台州318000 [2]浙江省台州医院,浙江台州317000

出　　处：《中国现代应用药学》2005年第z1期635-637,共3页Chinese Journal of Modern Applied Pharmacy

摘　　要：目的检出羚羊角和山羊角、羚羊角胶囊掺骨塞的真伪及钙含量。方法采用一般鉴别法,显微横切面鉴别法,紫外光谱法鉴别羚羊角和山羊角、羚羊角胶囊的真伪及EDTA法检测羚羊角胶囊中钙的含量。结果显微横切面鉴别和紫外光谱比较均能区别羚羊角与山羊角、羚羊角胶囊的真伪,在200nm^400nm波长处均有不同吸收;EDTA法则定,结果羚羊角和山羊角无钙成分,骨塞含钙为21.16%,两批胶囊分别含钙为7.28%~8.15%,折算成骨塞分别为34.26%~38.52%。结论方法简单、实用、迅速、准确。OBJECTIVE To detect the true and the false of comu saigae tataricae(CST) and comu capra hircus(CCH) and cornu saigae tataricae capsules(CSTC) and of the bone adulterant and of the calcium content in CSTC.METHODS The true and the false of CSTand CCH and bone adulterant in CSTC was detected by the Microscopical transverse sections identification and the ultraviolet spectra and the calcium in CSTC by the comparison of the genera differentiaiton and calcium concont by EDTA.RESULTS Methods of the Microscopical transverse setions identification and uitra-violet spectra showed varie-degree absorption at 200 ~400nm,which could distinguish the true and the false of CST and CCH and CSTC;the results of EDTA detection showed that the control medicinal material CST and CCH had no calcium copmonet but the bone adulterant contained calcium of 21.16%,and the two batches of CSTC cotained calcium of 7.25%and 8.15%Respectively.Which were converted into bone adulterant of 34.26%and 38.52%Respectively.CONCLUSION The methed is simple,practical,rapid and accurate.

关 键 词：羚羊角 山羊角 羚羊角胶囊 鉴别 钙含量 

分 类 号：R931.5[医药卫生—生药学]