Synthesis of La^(3+) and Nd^(3+) co-doped yttria nanopowder for transparent ceramics by oxalate precipitation method  被引量:4

Synthesis of La^(3+) and Nd^(3+) co-doped yttria nanopowder for transparent ceramics by oxalate precipitation method

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作  者:王能利 张希艳 邱关明 孙海鹰 刘全生 米晓云 王晓春 

机构地区:[1]School of Materials Science and Engineering,Changchun University of Science and Technology

出  处:《Journal of Rare Earths》2010年第2期232-236,共5页稀土学报(英文版)

基  金:supported by the Science and Technology Development Program of Jilin Province (20080511)

摘  要:Polycrystalline Nd3+ and La3+ co-doped yttria nanopowder Nd3+:Y1.90La0.10O3 for transparent ceramics was synthesized by co-precipitation method using oxalate acid as the precipitant and(NH4)2SO4 as the electrical stabilizer under ultrasonic radiation.Nanopowders calcined at different temperatures were characterized with thermal gravimetric-differential thermal analysis(TG/DTA),X-ray diffraction(XRD),transmitting electron microscopy(TEM),energy dispersive spectrometry(EDS) and spectral analysis techniques.Th...Polycrystalline Nd3+ and La3+ co-doped yttria nanopowder Nd3+:Y1.90La0.10O3 for transparent ceramics was synthesized by co-precipitation method using oxalate acid as the precipitant and(NH4)2SO4 as the electrical stabilizer under ultrasonic radiation.Nanopowders calcined at different temperatures were characterized with thermal gravimetric-differential thermal analysis(TG/DTA),X-ray diffraction(XRD),transmitting electron microscopy(TEM),energy dispersive spectrometry(EDS) and spectral analysis techniques.Th...

关 键 词:yttria nanopowder LANTHANA OXALATE CO-PRECIPITATION transparent ceramics rare earths 

分 类 号:TQ174.1[化学工程—陶瓷工业]

 

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