一种简单合成7-羟基-高异黄酮的催化方法  

A Concise Synthesis of 7-Hydroxy-homoisoflavonoid Catalytic Methods

作　　者：方旭兵[1] 高莹[1] 聂光辉[1] 温超[1] 戴康[1] 

机构地区：[1]中南民族大学药学院,湖北武汉430074

出　　处：《精细化工中间体》2012年第1期46-48,共3页Fine Chemical Intermediates

摘　　要：以间苯二酚和苯丙酸为原料,三氟化硼乙醚为催化剂合成了2',4'-二羟基二氢查尔酮(收率84%),再经过增碳成环得到7-羟基-高异黄酮(收率84%)。此法绿色简捷,生产成本较低。A general and single step synthesis of 7-hydroxy-homoisoflavonoid from the resorcinol and Phenypropionate using BF3-Et2O is described,The process gave the product in an overall yield of 84%.It is a novel green ang low-cost method for synthesis.

关 键 词：高异黄酮 三氟化硼乙醚 增碳环合 

分 类 号：TQ244[化学工程—有机化工]