新型层状钙钛矿化合物(CuCl)LaTiO_4的XRD分析  

XRD analysis of a new layered perovskite compound(CuCl)LaTiO_4

作　　者：魏宁[1] 高艳阳[1] 王金霞[1] 姚瑞霞[1] 

机构地区：[1]中北大学理学院化学系,山西太原030051

出　　处：《化工中间体》2012年第1期50-52,共3页

摘　　要：咪唑-1-乙酸乙酯水解制备出咪唑乙酸2,收率79%,进一步与苯甲醇进行酯化反应,合成出咪唑-1-乙酸苄酯1,收率42%,产品结构经过1HNMR表征。A new layered perovskite compound(CuCl) LaTiO_4 was prepared by hydrothermal method with NaLaTiO4 and CuCl_2 2H_2O as raw materials.The crystal structure of the product was characterized by XRD.The analysis showed that the(CuCl) LaTiO4 had Aurivillius phase perovskite structure,belonged to tetragonal crystal lattice,and had I4/mmm space group,in which unit cell parameters were:a = 3.87,c = 21.58

关 键 词：水解 酯化 咪唑-1-乙酸苄酯 制备 表征 

分 类 号：TQ252.3[化学工程—有机化工]