水热法合成纳米硫化锌  

The hydrothermal synthesis of ZnS nano-particles

作　　者：温玲玲[1] 王浩[1] 胡秀娟[1] 马亚娟[1] 

机构地区：[1]兰州交通大学化学与生物工程学院,兰州730070

出　　处：《化工中间体》2012年第2期34-36,共3页

摘　　要：采用水热法以氯化锌、氢氧化钠和硫代乙酰胺为原料,制备ZnS纳米粒子。通过XRD、TEM、IR吸收光谱和UV-vis吸收光谱表征了ZnS纳米粒子的形貌、尺寸和结构。结果表明,制备的纳米ZnS分散良好、平均粒径为12nm,且为球形粒子。ZnS nano-particles were hydrothermally synthesized at low-temperature using ZnCl2 and C2H5NS. The size, morphology and crystal data of the nano-zinc sulfide were analyzed by X-ray diffraction (XRD), transmission electron microscopy (TEM), Fourier transform infrared spectrometry (FT-IR) and UV-visible spectrophotometer. The results show that the nano-zinc sulfide particles are spherical and their average size is about 12 nm.

关 键 词：纳米材料 水热法 ZNS 

分 类 号：O614.24+1[理学—无机化学]