304不锈钢表面激光熔覆Ni60/石墨/MoS_2复合涂层组织  

Microstructure of Ni60 / graphite / MoS_2 composite layer on surface of304 stainless steel by laser cladding

作　　者：冯爱新[1,2] 吕豫文[2] 王术新[2,3] 薛伟[1] 裴绍虎[2] 章正刚[2] 曹宇鹏[2] 李峰平[1] 

机构地区：[1]温州大学机电工程学院,浙江温州325035 [2]江苏大学机械工程学院,江苏镇江212013 [3]镇江船艇学院,江苏镇江212013

出　　处：《材料热处理学报》2015年第4期189-194,共6页Transactions of Materials and Heat Treatment

基　　金：国家自然科学基金(51175237;51305050);"高档数控机床与基础制造装备"科技重大专项(2013ZX04009031-4);浙江省国际科技合作专项(2013C14007);江苏省"六大人才高峰"A类项目;中俄双边2014-2015政府间科技合作项目(CR17-11)

摘　　要：针对国内核电站再热双阀组阀杆表面乙炔气堆焊Co Cr W制备耐磨焊层无法满足60年服役寿命要求的问题,在阀杆材料(304不锈钢)表面激光熔覆Ni60/石墨/Mo S2复合涂层。采用X射线衍射(XRD)、扫描电镜(SEM)和显微硬度检测等技术研究了熔覆层组织结构、相组成、显微硬度。结果表明,试样C2熔覆层从底部到顶部,熔覆层晶体依次为:平面晶、胞状晶、胞-树枝状晶、柱状树枝晶、等轴树枝晶,且平均硬度最高,为990 HV0.3。随着激光功率的升高,各类熔覆层硬度的波动幅度逐渐减小,硬质相的分布也随之越来越均匀。Based on the consideration that the reheat double valve stem with Co Cr W coating by acetylene gas welding used in nuclear power plant failures to meet the requiments of 60-year service time,compose layers of Ni60 / graphite / Mo S2 on the 304 stainless steel stem surface were prepared by laser cladding using different formulation of the alloy powders. Microstructure,phase composition and microhardness of the clad layers were studied by means of X-ray diffraction( XRD),scanning electron microscopy( SEM) and microhardness test. The results show that there are flat crystal,cellular dendrite,columnar dendrites and equiaxed dendrites successively distributed from bottom to top of sample C2,and the average hardness of the sample C2 reaches the maximum value of about 990 HV0. 3. As the laser power increases,the fluctuation range of the hardness of the clad coating gets smaller and the distribution of hard phases is more uniform.

关 键 词：激光熔覆 304不锈钢 复合粉末涂层 微观组织 

分 类 号：TG174.4[金属学及工艺—金属表面处理]