高效循环电弧放电法制备大量单壁纳米碳管的研究  

The study on the efficient method for producing large amount of single-walled carbon nanotubes with recirculated arc discharge

作　　者：王新庆[1] 王淼[1] 李振华[2] 刘子阳[3] 

机构地区：[1]浙江大学物理系 [2]浙江大学力学系,杭州310027 [3]浙江大学化学系,杭州310027

出　　处：《物理学报》2004年第7期2254-2257,共4页Acta Physica Sinica

基　　金：国家自然科学基金 (批准号 :60 2 710 0 9);浙江省自然科学基金 (批准号 :5 0 110 9)资助的课题~~

摘　　要：介绍一种利用电弧放电法高效率制备大量单壁纳米碳管的新方法 .以钨代替传统的石墨棒作为放电阴极 ,采取循环式往返放电法 .同时利用高分辨透射电子显微镜及拉曼光谱对制备的单壁纳米碳管进行了观察、表征 .实验证明 :以钨为阴极的循环电弧放电法可以初步实现单壁纳米碳管的高效率、大批量生产 .By using Y-Ni-C composite rod as cathode, large amount of single-walled carbon nanotubes was produced by an improved arc discharge method, in which a tungsten rod was used as an electrode and the electrodes were exchanged after each discharge. The raw soot was characterized by high resdution electron microscope and Raman spectrum, and the results show that this is an efficient way to produce large amount of single-walled carbon nanotubes.

关 键 词：单壁纳米碳管 钨电极 拉曼光谱 高效循环电弧放电法 

分 类 号：TB383[一般工业技术—材料科学与工程]