催化合成对羟基苯甲酸丁酯的研究  

Study on catalytic synthesis of p-hydroxybenzoate

作　　者：姚春凤[1] 赵桂兰[1] 高志红[1] 

机构地区：[1]华南师范大学化学系,广东广州510631

出　　处：《应用化工》2004年第4期35-36,共2页Applied Chemical Industry

摘　　要：研究了FeCl3·6H2O为催化剂催化合成对羟基苯甲酸丁酯。讨论了催化酯化的各种影响因素,优化的反应条件为:对羟基苯甲酸与丁醇摩尔比为1∶3,催化剂与对羟基苯甲酸的摩尔比为0.04∶1,反应时间2.0h,对羟基苯甲酸丁酯产率为98.9%。The synthesis of butyl p-hydroxybenzoate with ferric chloride as catalysts was studied. the effects of reaction conditions were investigated ,the optimum were determined as follows:the molar ratio of p-hydroxybenzoic acid to butanol is 1∶3,the molar ratio catalyst to p-hydroxybenzoic acid is (0.04∶1),the reaction time is 2.0 h,the yield of butyl p-hydroxybenzoate is 98.9%.

关 键 词：对羟基苯甲酸丁酯 三氯化铁 催化 合成 

分 类 号：O621.25[理学—有机化学]