九龙胃药胶囊质量标准研究  

Study on Quality Standard for Jiulongweiyao Capsules

作　　者：蒋珍藕 陈荣光[2] 

机构地区：[1]广西天然药物研究中心,广西南宁530022 [2]广西中医药研究所,广西南宁530022

出　　处：《中国中医药信息杂志》2004年第7期607-609,共3页Chinese Journal of Information on Traditional Chinese Medicine

摘　　要：目的建立九龙胃药胶囊的质量标准。方法采用薄层色谱法鉴别九里香、肿节风、白芍;采用高效液相色谱法测定异嗪皮啶的含量。结果在薄层色谱中可检出九里香、肿节风、白芍;异嗪皮啶在0.0544～0.4896μg范围内与峰面积呈良好的线性关系,r=0.9997,平均回收率为98.76%,RSD=1.56%。结论所建立的方法可用于该制剂的质量控制。Objective To establish the quality control standard of Jiulongweiyao Capsules. Methods Folium et cacumen Murrayae, Herb Sarcandrae, Radix Paeonae Alba in Jiulongweiyao Capsules were identified by TLC. The content of isofraxidin in Jiulongweryao Capsules was determined by HPLC. Results Folium et cacumen Murrayae, Herb Sarcandrae, Radix Paeonae Alba could be detected by TLC. Isofraxidin showed a good linear relationship at range of 0.0544～0.4896 μg, r =0.9997. The average recovery was 98.76%, and RSD was 1.56%. Conclusion The established methods are accurate, reproducible and can be used for the quality control of Jiulongweiyao Capsules.

关 键 词：九龙胃药胶囊 异嗪皮啶 薄层色谱法 高效液相色谱法 质量标准 

分 类 号：R284.1[医药卫生—中药学]