骨松康胶囊中乌头碱含量测定  

Determination of Aconitine in Gusongkang Capsules

作　　者：彭天吉 林天慕[2] 王长海[2] 蒋永培[2] 邹帆 

机构地区：[1]东莞市中医院,东莞523079 [2]第四军医大学西京医院 [3]东莞中医院

出　　处：《中国药师》2004年第11期854-855,共2页China Pharmacist

摘　　要：目的 :建立骨松康胶囊中的乌头碱的含量测定方法。方法 :用异羟肟酸反应 高氯酸铁显色分光光度法测定骨松康胶囊及川乌、草乌药材中乌头碱的含量。结果 :该方法显色稳定性好 ,结果准确 ,回收率为 97.7% (RSD =2 .3% )。结论 :采用本法可较好地反映药品脱毒处理的水平 。Objective: To establish a method for determination of aconitine in Gusongkang capsules Method: Aconitine in Gusongkang capsules,Aconitum Carmichaeli and Aconitum kusnezoffii were determine by spectrophotometric of hydroxamic acid iron perchloric color reaction.Result: The method had a good stability color reaction and result, the average recovery of added sample and RSD were 97.7% and 2.3% , respectively.Conclusion: The method is simple and fast, and can be used for the quantitative analysis of aconitine, and insure safety and efficiency.

关 键 词：骨松康 乌头碱 异羟肟酸反应-高氯酸铁显色 

分 类 号：R927.2[医药卫生—药学]