心痛宁胶囊中皂苷类成分TLC指纹图谱的研究  

TLC fingerprint of Xintongning Capsules

作　　者：王隶书[1] 程东岩[1] 李阳[2] 

机构地区：[1]吉林省中医中药研究院,吉林长春130021 [2]吉林工业大学医院,吉林长春130022

出　　处：《中成药》2004年第11期864-866,共3页Chinese Traditional Patent Medicine

摘　　要：目的 :用薄层扫描法建立心痛宁胶囊中皂苷类成分的指纹图谱分析方法。方法 :采用硅胶G薄层板 ,以氯仿 醋酸乙酯 甲醇 水 (1 5∶4 0∶2 2∶1 0 ) 1 0℃以下放置过夜分层的下层溶液为展开剂 ,1 0 %硫酸乙醇溶液喷雾显色。以人参皂苷Rg1为参照物。结果 :共有 5个共有斑点。结论 :方法准确、可靠 ,可更好地控制心痛宁胶囊的内在质量。AIM: To set up a fingerprint analysis of Xintongning Capsules (Radix Notogenseng......) by TLC. METHODS: Silica gel G plate was adopted with developing underlayer of chloroform ethylacetate methanol water (15:40:22:10) under 10℃ resting overnight, 10% solution of H 2SO 4 in ethanol sprayed with and ginsenosides Rb 3 was used as standard substance. RESULTS: The result had 5 common spots. CONCLUSION: This method is accurate, reliable and provides a means for controlling the qualities of Xintongning Capsules.

关 键 词：心痛宁胶囊 指纹图谱 薄层扫描法 

分 类 号：R284.1[医药卫生—中药学]