无溶剂微波辐射合成双缩二氨基硫脲类化合物  

Microwave-Enhanced Synthesis of Thiocarbonohydrazones under Solvent-Free Conditions

作　　者：白银娟[1] 路军 杨玲[1] 师蔚鹏[1] 史真[1] 

机构地区：[1]西北大学化学系,西安710069

出　　处：《有机化学》2004年第11期1472-1474,共3页Chinese Journal of Organic Chemistry

基　　金：陕西省教育厅专项基金 (No.0 1JK2 0 5)资助项目 .

摘　　要：在无催化剂无溶剂微波辐射下用芳香醛和 1,3 二氨基硫脲合成了双缩二氨基硫脲类化合物 ,为该类化合物提供了一种新的简便合成方法 .The microwave-enhanced synthesis of thiocarbonohydrazones from aromatic aldehydes and thiocarbonohydrazide under solvent-free conditions without catalyst was achieved. This method is a good option to obtain the title compounds in a simple and inexpensive way. Their structures were confirmed by 1H NMR and IR spectra.

关 键 词：无溶剂微波辐射 双缩二氨基硫脲类化合物 合成 芳香醛 1 3-二氨基硫脲 

分 类 号：O623[理学—有机化学]