苯菌灵在葡萄中的残留量分析  

RESIDUE DETERMINATION OF BENOMYL IN GRAPES

作　　者：王鸣华[1] 毛国平[1] 杨春龙[1] 邢月华[1] 蒋木庚[1] 

机构地区：[1]南京农业大学基础课部,210014

出　　处：《南京农业大学学报》1993年第3期55-58,共4页Journal of Nanjing Agricultural University

摘　　要：苯菌灵提取物经酸性水解定量地转化为多菌灵,中和后用乙酸乙酯萃取,高效液相色谱定量测定。苯菌灵在葡萄中的平均添加回收率为100.69%,检测极限为0.01mg/kg。在南京和西安两地的试验结果显示,苯菌灵在葡萄上的半衰期为9.6和18.1d,最终残留量分别为0.70和1.19 mg/kg,喷药2次的最终残留量分别为1.78和2.66 mg/kg。A method for residue determination of benomyl in grape with high performance liquidchromatography (HPLC) was developed.The benomyl was quantitatively converted into carbendazim by acidhydrolysis.Neutralized to pH 10～11 with sodium hydroxide,the carbendazim was extracted with ethylacetate.After due concentration,the extract was analyzed by HPLC with UV detection at 285nm.Theaverage recovery was 100.69%.The minimum detectable level was 0.01mg/kg.The half life of benomyldeposit in grapes was 9.6d(Nangjing) and 18.1d (Xi'an),and the postharvest residues were 0.7mg/kg and1.19mg/kg,demonstrating that the benomyl residue is safety for consumers.

关 键 词：苯菌灵 葡萄 残留量 

分 类 号：S481.8[农业科学—农药学]