530μm大口径石英毛细管柱用于苯乙烯生产中的控制分析  

Control Analysis in Styrene Production by Wide Bore Fused Silica Capillary Gas Chromatography

作　　者：赵国宏[1] 吕祖芳[1] 刘岭[2] 朱绍康 

机构地区：[1]中国科学院兰州化学物理研究所,兰州730000 [2]兰州化学工业公司合成橡胶厂,兰州730060

出　　处：《石油化工》1993年第3期187-190,共4页Petrochemical Technology

摘　　要：用530μm交联SE-54大口径石英毛细管柱及拟柱上(at-column)进样技术,完成高纯苯乙烯中微量杂质的快速分析,一次分析只需12min。各微量杂质分析结果的精密度及准确度都较好,二乙烯基苯的检出限达10ppm。A styrene sample can be analyzed rapidly by wide bore (i. d. 530μm)fused silica capillary column within 12 minutes. The analysis time is about an hour faster than that of classical packed column. The stationary phase of the column is cross-linking SE-54. The precision and accuracy of data obtained by this method are same as that by classical packed column. The detection limit of divinylbenzene is 10ppm.

关 键 词：气相色谱 苯乙烯 毛细管柱 分析 

分 类 号：TQ241.21[化学工程—有机化工]