五氯吡啶的合成工艺优化  

Optimization of synthetic technology condition for pentachloropyridine

作　　者：许柳松[1] 曾作祥[1] 薛为岚[1] 吴超[1] 

机构地区：[1]华东理工大学化工学院,上海200237

出　　处：《应用化工》2005年第1期43-44,共2页Applied Chemical Industry

摘　　要：对五氯吡啶的合成工艺条件采用正交设计法进行了研究。优化的条件为:气空速500h-1,液空速0.070h-1,温度610K,时间24h。五氯吡啶的收率达到96.90%。The reaction condition for synthesizing pentachloropyridine were optimized with orthogonal design. The optimal technology condition are also determined.The result shows that the yield of pentachloropyridine is 96.90%, when gaseous phase space velocity is 500 h^(-1), liquid-phase space velocity is 0.070h^(-1), temperature is 610K,and time is 24 h.

关 键 词：五氯吡啶 吡啶 氯化 正交设计 

分 类 号：TQ203[化学工程—有机化工]