叔丁酚醛硫化树脂的合成研究  

Synthesis of tert - Butyl Phenolic Curing Resin

作　　者：张金菊[1] 

机构地区：[1]太原化学工业集团公司设计研究院,太原030021

出　　处：《精细石油化工进展》2005年第2期38-40,共3页Advances in Fine Petrochemicals

摘　　要：以六亚甲基四胺为催化剂,以对叔丁基苯酚和甲醛为原料,合成了叔丁酚醛硫化树脂。确定了最佳合成条件:反应温度94-98℃,反应时间3h,催化剂用量(以原料对叔丁基苯酚质量计)1.5%。制得的树脂颜色浅,软化点范围大,使得树脂的应用领域扩大。合成过程中操作稳定,且工艺流程简单。tert - Butyl phenolic curing resin was synthesized from p - ten - butylphenol and formaldehyde with methenamine as catalyst. The optimum reaction conditions were determined as follows: reaction temperature 94 -98 ℃ , reaction time 3 h, amount of catalyst 1.5 % (based on the mass of p - ten - butylphenol) . The product had light colour and wide range of softening point. The application field of the product was larger. The operation process was simple and stable.

关 键 词：树脂 酚醛 对叔丁基苯酚 合成研究 硫化 催化剂用量 合成过程 亚甲基 合成条件 反应温度 

分 类 号：TQ323.1[化学工程—合成树脂塑料工业]