Synthesis and Crystal Structure of N-Methyl-9-(3,4-dimethoxylphenyl)-1,8-dioxo-1,2,3,4,5,6,7,8,9,10- decahydroacridine under Microwave Irradiation  

作　　者：ZHANGXiao-Jing TUShu-Jiang ZHUXiao-Tong ZHANGJin-Peng XUJia-Ning WANGQian 

机构地区：[1]DepartmentofChemistry,XuzhouNormalUniversity [2]KeyLabofBiotechnologyforMedicinalPlantsofJiangsuProvince,Xuzhou,Jiangsu221009,China

出　　处：《Chinese Journal of Structural Chemistry》2005年第2期131-134,共4页结构化学（英文）

基　　金：The project was supported by the National Natural Science Foundation of China (No. 20372057); Natural Science Foundation; of Jiangsu Province (No. BK.2001142); the Open-end Fund of the Key Experiments of Organic Synthesis; Jiangsu Province; (S8109111) ; the Fund of Jiangsu Provincial Key Lab of Biotechnology for Medicinal Plants (01AXL 14)

摘　　要：The crystal structure of the title compound (C26H33NO4 (C25.68H32.04N0.68O4.32, Mr = 419.35)) has been determined by single-crystal X-ray diffraction. The crystal is of triclinic, space P21/c with a = 7.519(2), b = 28.933(5), c = 10.654(3) ?, β = 91.78(2)°, V = 2316.7(7) ?3, Z = 4, Dc = 1.202 g/cm3, μ = 0.081 mm-1, F(000) = 902, Mr = 423, the final R = 0.0424 and wR = 0.0911. In the structure, the pyridine ring adopts a boat conformation.The crystal structure of the title compound (C26H33NO4 (C25.68H32.04N0.68O4.32, Mr = 419.35)) has been determined by single-crystal X-ray diffraction. The crystal is of triclinic, space P21/c with a = 7.519(2), b = 28.933(5), c = 10.654(3) ?, β = 91.78(2)°, V = 2316.7(7) ?3, Z = 4, Dc = 1.202 g/cm3, μ = 0.081 mm-1, F(000) = 902, Mr = 423, the final R = 0.0424 and wR = 0.0911. In the structure, the pyridine ring adopts a boat conformation.

关 键 词：ACRIDINE MICROWAVE crystal structure 

分 类 号：O626.326[理学—有机化学] O76[理学—化学]