糙叶败酱挥发油成分的分离与鉴定  

Isolation and identification of the constituents of volatile oil from the Chinese drug Cao Ye Bai Jiang,rhizome and root of Patrinia scabra Bunge

作　　者：田珍[1] 陈战松[2] 楼之岑[1] 梁伟升[3] 庞吉海[3] 

机构地区：[1]北京医科大学生药教研室 [2]北京医科大学生物教研室研究生 [3]北京医科大学波谱分析室

出　　处：《中国药学杂志》1989年第2期78-79,共2页Chinese Pharmaceutical Journal

摘　　要：糙叶败酱Pat rinia scabra Bge.的根与根茎的挥发油前人报告证明有镇静作用。作者对该挥发油采用了气-质联用方法，并结合快速柱层分离和经红外光谱及氢核磁共振光谱鉴定了其中5种成分，主成分为石竹烯，另有α-古芸烯、β-古芸烯、α-葎草烯及正十六烷。这些成分均为首次自该植物中分出并鉴定的。Five components were identified from thevolatile oil separated by stemdistillationof the dried rhizome and root of Patrinia seabra Bunge(family Valerianaceae)byGC-MS,and three of them were coufirm-ed by I R and NMR after further isolationby means of flash column chromatography.The main component was found to be cary-ophyllene,and the others were α-humulene,α-,β-gurjunene and hexadecane.The prese-nce of these compounds in the volatile oilof this plant has not yet been reported pre-viously.

关 键 词：败酱 挥发油成分 首次 镇静作用 分离与鉴定 核磁共振光谱 氢核 石竹 葎草 根茎 

分 类 号：R284[医药卫生—中药学] R28[医药卫生—中医学]