三（β－氯乙基）磷酸酯的合成  

Synthesis of Tris (β-chloroethyl-)phosphate

作　　者：姬学仪 朱德湘[1] 

机构地区：[1]南京电化厂,南京化工学院

出　　处：《江苏化工》1994年第1期15-17,52,共4页Jiangsu Chemical Industry

摘　　要：以三氯氧磷和环氧乙烷为原料，在三组份催化剂（ＪＣ－１）的催化下合成三（β－氯乙基）磷酸酯，产品的纯度和收率都高。探讨了影响产率的几个因素，工艺简便，易于工业化。Tris (β-chloroethyl ) phosphate was synthesized from phosphorus oxychloride and epoxy ethane in the presence of three components catalyst (JC-1). The purity and yield of the product is high.The effect of ratio of amont of raw materials, temperature during feeding, and speed of stirring on yield was studied. The process is simple and easy to industrialize.

关 键 词：氯乙基 三磷酸酯 三氯氧磷 

分 类 号：TQ265.1[化学工程—有机化工]