新型阻燃剂Thermolin101的合成及应用  

Synthesis and Application of a New Flame Retardant Thermolin 101

作　　者：朱广军[1] 

机构地区：[1]南京理工大学化工学院

出　　处：《石油化工》1994年第8期527-531,共5页Petrochemical Technology

摘　　要：报道了由ＰＯＣｌ＿３、乙二醇和环氧乙烷反应合成阻燃剂Ｔｈｅｒｍｏｌｉｎ１０１的新合成路线。研究了影响反应的因素，反应收率可达到９０％。经红外光谱、核磁共振和元素分析测定了产品的化学结构，并做了在聚氨酯软泡中的应用试验，和阻燃涂层试验，结果显示Ｔｈｅｒｍｏｌｉｎ１０１是一种较好的新型阻燃剂。In this paper a new synthesis method for flame retardant Thermolin 101 from POCl_3,glycol and ethylene oxide was reported. The factors which influence the reaction werestudied.The yield reaehed 90%. The chemical structure of the product was exalnined byusing IR, NMR and elemental analysis.Application test in soft polyurethane foam and flameretardant coating test were made. It shows Thermolin 101 is a new good flame retardant.

关 键 词：阻燃剂 环氧乙烷 合成 乙二醇 

分 类 号：TQ314.248[化学工程—高聚物工业]