TiO_2纳米管负载Ag、Au、Pt纳米粒子的微波合成与表征  被引量:29

Microwave Synthesis and Characterization of Ag, Au, Pt Nanoparticles Supported on TiO_2 Nanotubes

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作  者:包华辉[1] 徐铸德[1] 殷好勇[1] 郑遗凡[1] 陈卫祥[1] 

机构地区:[1]浙江大学化学系,杭州310027

出  处:《无机化学学报》2005年第3期374-378,共5页Chinese Journal of Inorganic Chemistry

基  金:国家自然科学基金资助项目(No.20171039;50171063);教育部回国留学人员启动基金(2004-527)

摘  要:TiO2 nanotubes were prepared under normal pressure at a temperature of 120 ℃. Ag, Au, Pt nanoparticles supported on TiO2 nanotubes were prepared by m icrowave assisted heating polyol process. TEM images showed that microwave prepa red Ag, Au, Pt nanoparticles supported on TiO2 nanotubes were small and well dis persed on the surface of the TiO2 nanotubes. UV-Vis absorption spectra showed th at the absorbance of Ag/TiO2 nanotubes and Au/TiO2 nanotubes in the visible ligh t range increased greatly compared to the single titania nanotubes.TiO2 nanotubes were prepared under normal pressure at a temperature of 120 degrees C. Ag, An, Pt nanoparticles supported on TiO2 nanotubes were prepared by microwave assisted heating polyol process. TEM images showed that microwave prepared Ag, Au, Pt nanoparticles supported on TiO2 nanotubes were small and well dispersed on the surface of the TiO2 nanotubes. UV-Vis absorption spectra showed that the absorbance of Ag/TiO2 nanotubes and Au/TiO2 nanotubes in the visible light range increased greatly compared to the single titania nanotubes.

关 键 词:AU/TIO2 AG/TIO2 表征 微波合成 TIO2纳米管 UV-VIS 纳米粒子 负载 TEM 

分 类 号:O643[理学—物理化学]

 

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