消瘤胶囊的质量标准研究  

Quality Standard for Xiaoliu Capsule

作　　者：施亚芳[1] 魏惠华[1] 潘国梁[1] 范晨怡[1] 王勇[1] 

机构地区：[1]江苏省中医药研究院江苏省现代中药制剂工程技术研究中心,江苏南京210028

出　　处：《时珍国医国药》2005年第3期216-217,共2页Lishizhen Medicine and Materia Medica Research

摘　　要：目的:建立消瘤胶囊质量标准。方法:采用TLC法对黄芪、白芍进行了鉴别;用HPLC法测定芍药苷的含量。Zorbax C18柱;流动相:甲醇-水(40∶60);检测波长230nm。结果:TLC色谱斑点清晰。芍药苷在0.0282～0.1408mg/ml范围内呈良好的线形关系,平均加样回收率97.7%,RSD=1.1%。结论:所建立的方法简便可行,重现性好,为消瘤胶囊质量标准控制提供了方法。Objective:To establish a quality standard for Xiaoliu Capsule.Methods:Radix Astragall;Radix Paeoniae Alba in this medicine were identified by TLC.Paeoniflorin was determined by HPLC,using a Zorbax C 18column and CH 3OH:H 2O(40:60) as the mobile phase.The detection wavelength was 230 nm.Results:The TLC spots developed were clear.Paeoniflorin showed a good linear relationship at the range of 0.028 2～0.140 8 mg/ml.The average recovery of paeoniflorin was 97.7% and RSD was 1.1%.Conclusion:The method can be used for the quality control of Xiaoliu Capsule.

关 键 词：芍药苷 黄芪 白芍 质量标准 

分 类 号：R284.1[医药卫生—中药学]