Microwave-assisted Allylic Oxidation at C-13 Position of 14-Deoxysinenxan A  

作　　者：JunGU MengZHANG DaLiYIN JiYuGUO XiaoTianLIANG 

机构地区：[1]InstituteofMateriaMedica,ChineseAcademyofMedicalSciences＆PekingUnionMedicalCollege,Beijing100050

出　　处：《Chinese Chemical Letters》2005年第4期427-429,共3页中国化学快报（英文版）

基　　金：supported by NNSFC(grant No.30100230).

摘　　要：Microwave-assisted allylic oxidation at C-13 position of 14-deoxysinenxan A was described. This new method (150℃/10 min/5 bar on microwave synthesizer) led to a better yield of compound 1 and shorter reaction time.Microwave-assisted allylic oxidation at C-13 position of 14-deoxysinenxan A was described. This new method (150℃/10 min/5 bar on microwave synthesizer) led to a better yield of compound 1 and shorter reaction time.

关 键 词：Allylic oxidation MICROWAVE 14-deoxysinenxan A. 

分 类 号：R979.1[医药卫生—药品]