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机构地区:[1]山西省药品检验所,太原030001
出 处:《中国药品标准》2005年第1期46-46,57,共2页Drug Standards of China
摘 要:目的:改进枳壳中柚皮苷的含量测定方法。方法:比较样品提取中不过聚酰胺柱以及过不同粒度的聚酰胺柱的柚皮苷的含量,以确定最合适的方法。结果:聚酰胺粒度越细,有效成分损失越低,当粒度达到80~10 0目时,与未过柱的含量一致。讨论:样品处理不过聚酰胺柱或过80~10 0目是合适的方法。建议药典改进其方法。Objective:To improve the method of determination of Narrigin in Fructus Aurantii.Method:To establish the most appropriate method by comparing the content of Narrigin in sample which did not pass polyamide column and passed various granule grades polyamide columns.Results:The finer of granule grade of polyamide,the lower of loss of effective component.The content of Narrigin which passed 80~100 order of polyamide column is same with the content of Narrigin which did not pass polyamide column.Discussion:The most appropriate method is column.The method in pharmacopoeia should be improved.
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