活性炭吸附SnCl_4·5H_2O催化合成3-苯基丙烯酸甲酯  

Synthesis of methyl 3-phenylacrylate catalyzed by stannic chloride supported on activated carbon

作　　者：周勇[1] 林茹[1] 

机构地区：[1]平原大学化工系,河南新乡453003

出　　处：《应用化工》2005年第5期280-281,共2页Applied Chemical Industry

摘　　要：以活性炭SnCl4·5H2O为催化剂,合成了3 苯基丙烯酸甲酯,讨论影响反应的主要因素。得出最佳反应条件为:催化剂用量2.5g,3 苯基丙烯酸用量0.02mol,甲醇用量0.10mol,反应时间2.5h,酯的收率为90.2%。Synthesis of methyl 3-phenylacrylate catalyzed by stannic chloride supported on activated carbon was investigated. The optimum conditions are as follows: the amount of the catalyst is 2.5 g,the 3-phenylacrylic acid is 0.02 mol,the methanol is 0.1 mol,reaction time is 2.5 h,the yield of methyl 3-phenylacrylate is 90.2%.

关 键 词：3-苯基丙烯酸甲酯 活性炭 SNCL4·5H2O 酯化 

分 类 号：O623.624[理学—有机化学]