反胶束微乳液法合成纳米SrTiO_3研究  被引量:16

Study on Synthesis of Nano-crystalline SrTiO_3 by Inverse Micell Microemulsion Method

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作  者:李月峰[1] 赖琼钰[1] 

机构地区:[1]四川大学化学学院,成都610064

出  处:《无机化学学报》2005年第6期915-918,F011,共5页Chinese Journal of Inorganic Chemistry

基  金:四川省基础应用研究基金资助项目(No.川教科9902)

摘  要:The precursors of SrTiO3 were prepared by inverse micell microemulsion method. SrTiO3 nano-powders were synthesized by calcining the precursors at 800 ℃ in air for 4 hours and were characterized by XRD, IR, TG, SEM. The results show that the spherical SrTiO3 nano-particles have narrow distribution with an average size of 40 nm. The surfactants played an important role in controlling shape and size of nano-particles, and combined surfactants were more effective than single surfactant.The precursors of SrTiO3 were prepared by inverse micell microemulsion method. SrTiO3 nano-powders were synthesized by calcining the precursors at 800 degrees C in air for 4 hours and were characterized by XRD, IR, TG, SEM. The results show that the spherical SrTiO3 nano-particles have narrow distribution with an average size of 40 nm. The surfactants played an important role in controlling shape and size of nano-particles, and combined surfactants were more effective than single surfactant.

关 键 词:反胶束微乳液法 表面活性剂 合成 纳米晶 钛酸锶 电子陶瓷材料 

分 类 号:O614.232[理学—无机化学] TB383[理学—化学]

 

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