间苯二腈中的苯甲腈、间甲苯甲腈气相色谱法分析  

Analysis of m-Phthalodinitrile by Gas Chromatography

作　　者：孙伟 王培建 付越 

机构地区：[1]山东大成农药股份有限公司,淄博255009

出　　处：《精细化工原料及中间体》2005年第7期31-32,共2页Fine Chemical Industrial Raw Materials & Intermediates

摘　　要：用气相色谱仪1.5%SP2250+2%QF-1色谱柱对苯甲腈,间甲苯甲腈两种组分同时进行定量分析(FID检测器)。内标选择正十五烷,该方法简便、快速、准确。本方法中苯甲腈,间甲苯甲腈的变异系数分别为0.37%和0.52%,回收率为99.86%和99.51%,线性相关系数分别为0.9997和0.9998。A method is introduced for quantitative determination of benzonitribe m-tolunitrile in m-phthalodinitrile by gas chromatograph on 1.5%SP2250+2%QF-1 chromatographic column and FID using n-pentadecane as internal standard. The method was simple, rapid and accurate. The resalts showed that the coefficient of variation,average recovery and linear correlation of benzonitribe and m-tolunitrile were 0.37%,99.86%,0.9997 and 0.52%,99.51%,0.9998 respectively.

关 键 词：气相色谱法分析 苯甲腈 间苯二腈 FID检测器 线性相关系数 气相色谱仪 定量分析 变异系数 色谱柱 回收率 

分 类 号：TQ246.7[化学工程—有机化工] TS47[农业科学—烟草工业]