双波长差示光谱法测定甲蓉片中丹皮酚的含量  被引量:6

Determination of Paeonol in Jia Rong Tablet by DifferentialDouble Wave-length UV Spectrophotometry

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作  者:王剑波[1] 陈波[1] 王晓娟[1] 

机构地区:[1]第四军医大学药物研究所,陕西中医学院药学系九○级

出  处:《中药新药与临床药理》1995年第1期54-56,共3页Traditional Chinese Drug Research and Clinical Pharmacology

摘  要:利用丹皮酚在碱性介质中紫外吸收光谱发生特征位移,用双波长差示先谱法消除干扰组分的影响,测定了甲蓉片中丹皮酚的含量。方法快速简便,结果准确,回归方程和相关系数分别为Y=0.00651+44.0289X,r=0.9996,加样回收率=102.42%,RSD%=0.87。为该药的质量控制提供了一种较好的定量方法。A method for the determination of paeonol content in JIA Rong Tablet was reportedBy applying the specific untraviolet absorption spectrum shift of paeonol in basic medium and thedifferential double wnve-length UV spectrophotometry, the influence of interfering components waseliminated. The method is easy and quick, and the result is reliable. The standard curve regressionequation was Y=0.00651+44.0289X, r=0.9996. The average recovery was 102.42% , RSD=0.87% (n=6).This method offers a better qualitative way to control the quality of JIA RONG tablet.

关 键 词:中药 甲蓉片 丹皮酚 分光光度测定法 化学分析 

分 类 号:R284.1[医药卫生—中药学]

 

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