除草剂解毒剂二氯乙酰胺合成的研究  

THE STUDY OF ANTIDOTE SYHTHESIS OF DICHLOROACETAMIDE COMPOUNDS

作　　者：叶非[1] 冯志彪[1] 徐宝荣[1] 葛蔚[1] 刘淑新 

机构地区：[1]东北农业大学基础部

出　　处：《东北农业大学学报》1995年第3期302-304,共3页Journal of Northeast Agricultural University

基　　金：黑龙江省自然科学基金

摘　　要：首次利用薄层色谱法（ＴＬＣ）研究３三个解毒剂的合成条件，确定了它们反应的最佳时间和产物的Ｒｆ值，用气相色谱对产物进行了定性的纯度分析．Dichloroacetamides have been selectively synthesized with dichloroacetylehloride and amine.A new method for analysing(TLC)was proposed, the conditions of reaction was detected.The effects of Structure,temperature and reaction time have been investigated.The reaction gave higher yield(90.5%)and shorter-time (4h).Rf value of product was first determined.

关 键 词：解毒剂 二氯乙酰胺 合成 除草剂 

分 类 号：S482.4[农业科学—农药学] TQ457.26[农业科学—植物保护]