Microwave-prompted Rapid and Efficient Synthesis of Diacyl Thiosemicarbazides and Semicarbazides in Solvent and Catalyst Free Condition  

作　　者：Xi Cun WANG Zheng Jun QUAN Man Gang WANG Zheng LI 

机构地区：[1]Gansu Key Laboratory of Polymer Materials, College of Chemistry and Chemical Engineering, Northwest Normal University, Lanzhou 730070

出　　处：《Chinese Chemical Letters》2005年第8期1027-1030,共4页中国化学快报（英文版）

基　　金：The authors thank the Scientific and Technological Innovation Engineering of Northwest Normal University(NWNU-KJCXGC-02-08);Natural Science Foundation of Gansu Province(ZS021-A25-006-Z);Environmental Protection Foundation of Gansu Province(GH2003-19)for the financial support of this work.

摘　　要：Eighteen 1-aroyl-4-（2-iodobenzoyl）thiosemicarbazides and corresponding semicarbazides were synthesized in excellent yield under microwave irradiation in solvent and catalyst free condition.Eighteen 1-aroyl-4-（2-iodobenzoyl）thiosemicarbazides and corresponding semicarbazides were synthesized in excellent yield under microwave irradiation in solvent and catalyst free condition.

关 键 词：Microwave irradiation 1 4-diaroyl thiosemicarbazides 1 4-diaroyl semicarbazides solvent-free synthesis. 

分 类 号：O623.663[理学—有机化学]