当归补血汤汤剂中挥发油成分的GC-MS分析  

GC-MS analysis of volatile oil of Danggui Buxue Decoction

作　　者：黄月纯[1] 黄水清[2] 刘东辉[2] 魏刚[3] 

机构地区：[1]广州中医药大学第一附属医,院广东广州510405 [2]广州中医药大学,广东广州510405 [3]广州中医药大学第一附属医院,广东广州510405

出　　处：《中成药》2005年第8期892-894,共3页Chinese Traditional Patent Medicine

基　　金：广东省中医药管理局资助课题(103025)

摘　　要：目的:探讨当归补血汤汤剂(黄芪、当归)中挥发油的主要成分。方法:采用GCMS方法分析挥发油主要组分。在进样口温度250℃,接口温度230℃,载气流速1.3mL·min-1,柱压为100kPa,升温速率3℃·min-1的色谱条件下,挥发油主成分可达到较好分离。结果:当归补血汤汤剂中挥发油的主要成分为反式藁本内酯、正丁烯基苯酞、正丁基苯酞、顺式藁本内酯等。结论:当归补血汤汤剂中挥发油成分主要来自当归挥发油成分。AIM ： To study the main components of volatile oil of Danggui Buxue Decoction （ Radix Astragali Radix Angelicae Sinensis） . METHODS ： The main components of volatile oil were determined by GC-MS. The injector temperature was 250℃. The interface temperature was 230℃. The column flow was 1.3 mL ·min^- 1. The column pressure was 100 kPa. The temperature rate was 3℃·min^-1. RESULTS： The main components of volatile oil of Danggui Buxue Decoction were composed of trans-ligustilide, butylidene phthalide, n-butylphthalide, and cis-ligustilide. CONCLUSION： The main components of volatile oil of Danggui Buxue Decoction come mainly from volatile oil of Radix Angelicae sinensis.

关 键 词：当归补血汤 挥发油 GC-MS 

分 类 号：R927.2[医药卫生—药学]