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作 者:杨欣[1] 董川[1] 魏雁声 晋卫军[1] 刘长松[1]
机构地区:[1]山西大学化学系
出 处:《高等学校化学学报》1996年第5期716-718,共3页Chemical Journal of Chinese Universities
基 金:国家自然科学基金;西省自然科学基金
摘 要:同步扫描-微乳状液增稳室温磷光法同时测定痕量多环芳烃的研究杨欣,董川,魏雁声,晋卫军,刘长松(山西大学化学系,太原,030006)关键词同步扫描-微乳状液增稳室温磷光法;化学除氧技术;多环芳烃1978年Vo-Dinh等[1]将固定波长同步扫描技术用于...In this paper,a new method of synchronous microemulsion stablized room temperature phosphorimetry for the simultaneous determination of fluoranthene and chrysene, fluoranthene and acenaphthene, fluoranthene and p-terphenyl is described. The experiments indicate that suitable △λare 188 nm, 185 nm and 191 nm in proper order. Synchronous peaks are situated at 360 nm and 323 nm(fluoranthene and chrysene), 360 nm and 306 nm(fluoranthene and acenaphthene), 360 nm and 307 nm(fluoranthene and p-terpheny1)respectively in the mixture. The limit quantity of interference between components in binary mixture was examined. The linear range of determination reached two amount order and relative standard deviation less than 5%. The results of determination for double components synthetic sample are satisfactory.
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