2,4,6-三巯基-1,3,5-三嗪三钠盐的制备  

Preparation of 2,4,6-trithione-1,3,5-triazine trisodium salt

作　　者：刘安昌[1] 余磊[1] 邹菁[1] 苏建宇[1] 

机构地区：[1]武汉化工学院化工与制药学院,湖北武汉430074

出　　处：《武汉化工学院学报》2005年第4期8-10,共3页Journal of Wuhan Institute of Chemical Technology

摘　　要：以三聚氯氰为原料,硫化钠为巯基化试剂,在温度为60～70 ℃,pH=9的条件下,制备了2,4,6-三巯基-1,3,5-三嗪(收率≥90%)及其三钠盐.并对制备的2,4,6-三巯基-1,3,5-三嗪和瑞士Fluka公司相同的产品进行了红外光谱分析.2,4,6 - trithione - 1,3,5 - triazine and its trisodium salt were synthesized from cyanuric chloride by sulfhylization with sodium sulfide at 60-70℃ ,maintaining the pH=9 by addition of NaOH aqueous solution. The yield of 2,4,6 - trithione - 1,3,5 - triazine is ≥90%, and its structure was identified by IR spectrum and the IR spectrum of 2,4,6 - trithione - 1,3,5 - triazine was consistent with the IR spectrum of Fluka product.

关 键 词：三聚氯氰 巯基化试剂 2 4 6一三巯基一1 3 5一三嗪 

分 类 号：F240[经济管理—劳动经济]