固体碱催化合成9-芴甲醇  

The Method of Synthesizing 9- Fluorenylmethanol By Solid Base Catalyst

作　　者：陈叶飞[1] 张秀云[1] 刘年金[1] 

机构地区：[1]上海宝钢化工有限公司技术中心,上海200942

出　　处：《上海化工》2005年第9期20-23,共4页Shanghai Chemical Industry

摘　　要：以安全价廉的固体碱为催化剂,采用“一锅法”工艺合成芴甲醇。芴甲醇产率为36.7%,同时可获得高纯度的副产物9,9-二羟甲基芴,未反应的芴可循环利用。该方法尚未见国内外文献报道。“A pot”process for synthesizing 9-fluorenylmethanol is developed by using safe and economic solid base catalyst. The yield of 9-fluorenylmethanol is 36.7%, at the same time, the 9,9-bis （hydroxymethyl） fluorene is gotten with high purity. The fluorene unreacted can be used again. The method has not been reported at home and abroad.

关 键 词：芴 芴甲醇 固体碱催化剂 合成 

分 类 号：TQ245[化学工程—有机化工]