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机构地区:[1]Department of Chemistry, Zhejiang University,Hangzhou 310027, China
出 处:《Journal of Zhejiang University-Science B(Biomedicine & Biotechnology)》2005年第8期719-721,共3页浙江大学学报(英文版)B辑(生物医学与生物技术)
基 金:Project (Nos. 20375036 and 20472073) supported by the NationalNatural Science Foundation of China
摘 要:1H-NMR and 13C-NMR assignments of 12-oleanene-3,11-dione (compound 1) were completely described for the first time through conventional 1D NMR and 2D shift-correlated NMR experiments using 1H-1HCOSY, HMQC, HMBC techniques. Based on its NMR data, the assignments of 28-hydroxyolean-12-ene-3,11-dione (compound 2) were partially revised.^1H-NMR and ^13C-NMR assignments of 12-oleanene-3,11-dione (compound 1) were completely described for the first time through conventional 1D NMR and 2D shift-correlated NMR experiments using ^1H-^1HCOSY, HMQC, HMBC techniques. Based on its NMR data, the assignments of 28-hydroxyolean-12-ene-3,11-dione (compound 2) were partially revised.
关 键 词:Euonymus hederaceus 12-oleanene-3 11-dione 28-hydroxyolean- 12-ene-3 11-dione 1D-NMR 2D-NMR Assignment
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