一类双羟基西夫碱化合物的合成及表征  

Synthesis and characterization of a series of dihydroxy-Schiff bases

作　　者：万有志[1] 张小强[1] 范慧[1] 

机构地区：[1]北京化工大学理学院,北京100029

出　　处：《北京化工大学学报（自然科学版）》2005年第5期78-80,共3页Journal of Beijing University of Chemical Technology(Natural Science Edition)

摘　　要：文中以1,6-己二醇或其它类二醇、对硝基酚、对醛基苯乙醇为主要原料,采用Williamson醚合成法和其它方法合成了一类新型西夫碱化合物,其通式为HO—C2H4—C6H4—CH N—C6H4—OCnH2nOH(n=2,3,4,5,6),重点研究了n=6时的西夫碱,并通过熔点测定1、H-NMR和IR等方法,对该西夫碱的结构进行了表征。With 1, 6-hexanediol and others, p-nitrophenol and etc. as the main materials, a series of new Schiff bases with a general formular of HO-C2H4-C6H4-CH=N-C6H4-OCnH2nOH（ n = 2～6） was synthesized by the Williamson method and others. The strueture of the synthesized Seiff base（ n = 6） was eharaeterized by the methods of melting point, ^1H-NMR and IR.

关 键 词：西夫碱 Williamson法 合成 

分 类 号：O625.632[理学—有机化学]