外消旋螺环二酮的合成工艺条件研究  

Study on the synthesis of spiro[4,4] monane-1,6-dione

作　　者：张毅[1] 韩晓燕[1] 郝金库[2] 

机构地区：[1]天津中医学院中药系,天津300193 [2]天津师范大学化生学院,天津300074

出　　处：《天津化工》2006年第1期17-19,共3页Tianjin Chemical Industry

基　　金：天津市自然科学基金(003602011);天津市教委基金资助项目(990710)

摘　　要：详细研究了以己二酸、溴代丁酸乙酯为原料,采用简便高效的方法制备外消旋螺环二酮的最佳条件和有关工艺。The synthetical methods of spiro [4,4] nonane-1,6-dione were studied in the article. Spiro [4,4] nonane-1,6-dione was prepared by efficient methods, and optimized and improved reaction condition has been given by a series of experiments.

关 键 词：螺环二酮 蒸馏 合成 

分 类 号：TQ234.2[化学工程—有机化工]