Synthesis of Novel 1-Arylsulfonyl-4-(1′-N-2′, 3′, 4′, 6′-tetra- O-acetyl-β-D-glucopyranosyl)thiosemicarbazides  

作　　者：Yu Xin LI Zheng Ming LI Wei Guang ZHAO Wen Li DONG Su Hua WANG 

机构地区：[1]State Key Laboratory of Elemento-Organic Chemistry, Nankai University, Tianjin 300071

出　　处：《Chinese Chemical Letters》2006年第2期153-155,共3页中国化学快报（英文版）

基　　金：supported by NNSFC(No.20432010);Tianjin Natural Science Foundation(No.033803411).

摘　　要：The synthesis of novel 1-arylsulfonyl -4- （1＇-N -2＇, 3＇, 4＇, 6＇-tetra-O-acetyl-β-D-gluco- pyranosyl） thiosemicarbazides via condensation of 2, 3, 4, 6-tetra-O-acetyl-β-D-glucopyranosyl isothiocyanate with substituted phenylsulfonyl hydrazines was described. Their structures and physical properties were confirmed by ^1H NMR, ^13C NMR spectra, elemental analysis and MS.The synthesis of novel 1-arylsulfonyl -4- （1＇-N -2＇, 3＇, 4＇, 6＇-tetra-O-acetyl-β-D-gluco- pyranosyl） thiosemicarbazides via condensation of 2, 3, 4, 6-tetra-O-acetyl-β-D-glucopyranosyl isothiocyanate with substituted phenylsulfonyl hydrazines was described. Their structures and physical properties were confirmed by ^1H NMR, ^13C NMR spectra, elemental analysis and MS.

关 键 词：Phenylfulfonyl hydrazine thiosemicatbazide condensation. 

分 类 号：O626.4[理学—有机化学]