吖嗪类化合物合成新方法——1-(间苯氧基苯基)-4-甲基-4-(对乙氧基苯基)-2-戊酮吖嗪的合成  

New Systhetic Method of Azine Compound——Synthesis of 1- (m-Phenoxypheny1)-4-Methyl-4- (p-Ethoxypheny1)-2-Pentartone Azine

作　　者：李应福[1] 王红军[2] 

机构地区：[1]安徽大学实验中心 [2]安徽大学化学系

出　　处：《安徽大学学报（自然科学版）》1990年第3期57-59,共3页Journal of Anhui University(Natural Science Edition)

摘　　要：本文报道用1-(间苯氧基苯基)-4-甲基-4-(对乙氧基苯基)-2-戊酮与85％水合胼直接反应来合成1-(间苯氧基苯基)-4-甲基-4-(对乙氧基苯基)-2-戊酮吖嗪的实验方法。The synthesis of 1-(m-phenoxyphenyt) -4-methyl-4-(p-ethoxypheny1)-2-pentanone azine by direct reating between 1-(m-phenoxypheny1)-4-methy1-4-(p-ethoxypheny1)-2-pentanone and 85% hydrazine was reported in the paper. The synthetic conditions and yields of this azine compound were studied under the designs of different material ratioes, ethanol as solvent and diethylene glycol as solvent. The structure of rite title compound was also confirmed by IR, NMR, MS and elemental analysis.

关 键 词：吖嗪化合物 水合肼 有机合成 

分 类 号：O626[理学—有机化学]