利用环糊精包结的醋酸镍制备NiO纳米粒子  

Preparation of NiO Nanoparticles via Thermal Decomposition of Nickel Acetate Coated by CDs

作　　者：赵斌[1] 杨阳[1] 包建华[1] 陈慧兰[1] 

机构地区：[1]南京大学化学化工学院配位化学国家重点实验室,南京210093

出　　处：《无机化学学报》2006年第5期952-956,共5页Chinese Journal of Inorganic Chemistry

基　　金：国家自然科学基金资助项目(No.50272029)

摘　　要：NiO nanoparticles are prepared via thermal decomposition of nickel acetate coated by β-CD, and Characterized by using X-ray diffraction (XRD), transmission electron microscopy (TEM). Thermo-gravimetric (TG) analysis and electro spray mass spectrum (ESI-MS) are performed to investigate the thermal decomposition process and the possible formation mechanism of obtaining good morphology NiO nanoparticles by this method. Further, different CDs are used to prepare the precursors of inclusion complexes, and there are little affect of CD′s type on the NiO nanoparticles.NiO nanoparticles are prepared via thermal decomposition of nickel acetate coated by β-CD, and Characterized by using X-ray diffraction （XRD）, transmission electron microscopy （TEM）. Thermo-gravimetric （TG） analysis and electro spray mass spectrum （ESI-MS） are performed to investigate the thermal decomposition process and the possible formation mechanism of obtaining good morphology NiO nanoparticles by this method. Further, different CDs are used to prepare the precursors type on the NiO nanoparticles. of inclusion complexes, and there are little affect of CD＇s

关 键 词：NiO纳米粒子 环糊精 醋酸镍 热分解 

分 类 号：O614.813[理学—无机化学]