四氯化锡催化乙酸戊酯的合成研究  

Study on the Catalytic Synthesis of Banana Oil by Tin Tetrachloride

作　　者：杨国臣[1] 薛万华[1] 

机构地区：[1]雁北师范学院化学系,山西大同037009

出　　处：《山西广播电视大学学报》2006年第3期106-107,共2页Journal of Shanxi Radio & TV University

摘　　要：用四氯化锡取代浓硫酸作为冰乙酸和正戊醇的酯化反应催化剂,成功地合成了乙酸戊酯。在探讨了酯化反应的历程后,找到了较好的反应条件:酸醇摩尔比为1、催化剂用量2.54%、反应时间为60m in,产率达89.9%。Tin tetrachloride can be used as catalyst for esterification reaction of acetic acid and n-amyl alcohol instead of sulfuric acid. The mechanism of the esterfication reaction and the effect on catalytic reaction were studied. The best conditions were found out： the yield of product can be up to 89.9% for 60 min, the molar ratio of acetic acid and n-amyl alcohol is 1：1.13 and catalyst is 2. 54%.

关 键 词：乙酸戊酯 四氯化锡 催化 合成 

分 类 号：D643.36[政治法律—政治学]