Synthesis and Structure Elucidation of New Spiro Compounds with Per（poly）fluoroalkyl Group  

作　　者：施志坚 倪华文 曹卫国 刘卫霞 梁超 

机构地区：[1]Department of Chemistry, Shanghai University, Shanghai 200444, China [2]Key Laboratory of Organofluorine Chemistry, Shanghai Institute of Organic Chemistry, Chinese Academy of Sciences, Shanghai 200032, China

出　　处：《Chinese Journal of Chemistry》2006年第7期980-982,共3页中国化学（英文版）

基　　金：Project supported by the National Natural Science Foundation of China （No. 20472047）.

摘　　要：A series of spiro compounds have been synthesized via several steps. The structure of these compounds were confirmed by ^1H NMR, 13C NMR, IR, MS spectra and X-ray diffraction analysis. The possible mechanism to form these products was also proposed.A series of spiro compounds have been synthesized via several steps. The structure of these compounds were confirmed by ^1H NMR, 13C NMR, IR, MS spectra and X-ray diffraction analysis. The possible mechanism to form these products was also proposed.

关 键 词：structure elucidation per（poly）fluoroalkylation reaction spiro compound 

分 类 号：O624.2[理学—有机化学]