高效液相色谱法鉴别黑色签字笔墨水字迹形成时间的研究  

Identification of the Aging of Black Signing-pen Ink Writing by High Performance Liquid Chromatography

作　　者：许英健[1] 史晓凡[1] 王彦吉[2] 王景翰[1] 李心倩[1] 

机构地区：[1]中国刑警学院法医系,辽宁沈阳110035 [2]中国人民公安大学,北京100038

出　　处：《分析测试学报》2006年第4期52-54,58,共4页Journal of Instrumental Analysis

基　　金：国家高技术应用部门发展项目(计高技20012492);公安部重点课题(200119300007)

摘　　要：采用高效液相色谱法对在室温暗处保存的不同形成时间的黑色签字笔墨水字迹色痕进行了分析,通过染料成分相对含量的变化来确定黑色签字笔墨水字迹色痕的相对形成时间;并且在强光灯及室内自然光下对黑色签字笔墨水字迹进行了人工老化处理,通过光照老化实验得出染料的变化规律,为字迹形成时间的鉴定奠定了基础。The identification of relative age of the ink entries written by the same black signing-pen on documents stored in different light conditions is presented. The documents were stored in darkness and exposed to daylight and artificial light from 500 W visible analyzer for quite a number of days, respectively. Inks were then extracted from the respective documents and analyzed by HPLC. The variations of the relative contents of the dye component in the ink extracted from the documents under different light conditions were further studied. The variation regularities of the dye component under different aging conditions thus obtained would be the basis for the identification of the aging time of the ink entries written by the black signing-pen on documents.

关 键 词：法庭科学 高效液相色谱法 黑色签字笔墨水 形成时间 光照老化 

分 类 号：O657.72[理学—分析化学]