FTIR监测7-氟-2H-1,4-苯并噁嗪-3(4H)-酮的固相合成  

Monitoring of Solid-phase Synthesis of 7-Fluoro-2H-1,4-benzoxazine-3(4H)-ones via FTIR Spectroscopy

作　　者：黄明智[1] 谌伟民[1] 黄可龙[2] 黄路[3] 杨光富 

机构地区：[1]华中师范大学化学系,武汉430079 [2]中南大学化学化工学院,长沙410083 [3]湖南化工研究院国家农药创制工程技术研究中心,长沙410007

出　　处：《高等学校化学学报》2006年第11期2117-2119,共3页Chemical Journal of Chinese Universities

基　　金：国家自然科学基金(批准号:20372021;B20572019)资助

摘　　要：The solid-phase synthesis of 7-fluoro-1,4-2H-benzoxazine 3(4H)-ones on Wang resin via esterification,etherification,reduction,cyclization and cleavage reactions was studied,and the reaction conditions were optimized after analyzing the reaction kinetics according to the IR spectrum.The solid-phase synthesis of 7-fluoro-1,4-2H-benzoxazine 3 （4H）-ones on Wang resin via esterification, etherification, reduction, cyclization and cleavage reactions was studied, and the reaction conditions were optimized after analyzing the reaction kinetics according to the IR spectrum.

关 键 词：组合化学 固相有机合成 红外光谱 

分 类 号：O621.3[理学—有机化学]