伏格列波糖中有机溶剂残留量的毛细管GC测定  

Determination of Residual Solvents in Voglibose by Capillary GC

作　　者：张斐[1] 李小敏[1] 涂秀芹[1] 许向阳[1] 陈峻崧[1] 

机构地区：[1]江苏先声药物研究有限公司,江苏南京210042

出　　处：《中国医药工业杂志》2006年第11期773-774,共2页Chinese Journal of Pharmaceuticals

摘　　要：建立了毛细管GC法测定伏格列波糖中11种有机溶剂的残留量。以50%DMF水溶液为溶剂,采用DB-624弹性石英毛细管柱,程序升温,FID检测器,载气为氮气。A temperature programmed capillary GC method for determination of eleven residual solvents in voglibose was established. Fifty percent DMF aqueous solution was used as the solvent. A DB-624 capillary column was used with FID detector, and using nitrogen as carrier gas.

关 键 词：伏格列波糖 有机溶剂残留 气相色谱 测定 

分 类 号：TQ460.77[化学工程—制药化工] O657.71[理学—分析化学]