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机构地区:[1]贵州大学化学工程学院,贵州贵阳550003 [2]贵州大学理化分析中心,贵州贵阳550003
出 处:《贵州工业大学学报(自然科学版)》2006年第5期15-18,共4页Journal of Guizhou University of Technology(Natural Science Edition)
摘 要:以烷基多苷、顺丁稀二酸酐为原料,对甲苯磺酸为催化剂,通过酯化、磺化反应合成了阴离子表面活性剂—烷基多苷磺基琥珀酸单酯二钠盐,探讨了各主要影响因素对合成反应过程及结果的影响。The disodlum alkyl polyglycoside sulfosuccinate was synthesized by esterifying and sulfonating reaction of alkyl polyglycoside, succnic acid in the presence of p- toluenesulfonic acid, and influence factors of the synthetic process were also studied. The optimum conditions obtained by experiment were as follows: esterifying temperature 95℃, sulfonating temperature 80℃, amount of catalys is 1.5 % (based on the weight of succnic acid) ,n (succnic acid) :n (APG) = 1.5:1. The yield was 45.64%.
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