An Expedient Method for the Synthesis of Thiosemicarbazones under Microwave Irradiation in Solvent-free Medium  

作　　者：李建平 郑鹏志 朱俊歌 刘锐杰 渠桂荣 

机构地区：[1]College of Chemistry and Environmental Science, Henan Normal University, The Key Laboratory of Environmental Pollution Control of Henan Province, Xinxiang, Henan 453007, China

出　　处：《Chinese Journal of Chemistry》2006年第12期1773-1776,共4页中国化学（英文版）

基　　金：Project supported by the National Natural Science Foundation of China （No. 20372018）.

摘　　要：A simple, efficient and eco-friendly method for the synthesis of thiosemicarbazones from thiosemicarbazides and aldehyde under microwave irradiation has been reported, and no solvent and catalyst were used. And the technique of microwave irradiation coupled with solvent-free condition proved to be a quite valuable method in the organic synthesis.A simple, efficient and eco-friendly method for the synthesis of thiosemicarbazones from thiosemicarbazides and aldehyde under microwave irradiation has been reported, and no solvent and catalyst were used. And the technique of microwave irradiation coupled with solvent-free condition proved to be a quite valuable method in the organic synthesis.

关 键 词：THIOSEMICARBAZONE THIOSEMICARBAZIDE ALDEHYDE microwave SOLVENT-FREE 

分 类 号：O623.8[理学—有机化学] O623.7[理学—化学]