乙酰氯法测定含环氧基聚酯羟值  

Determination of Hydroxyl Value of Epoxy-Containing Polyester by Acetyl Chloride Method

作　　者：朱小树[1] 

机构地区：[1]黎明化工研究院,河南洛阳471001

出　　处：《化学推进剂与高分子材料》2007年第1期65-66,共2页Chemical Propellants & Polymeric Materials

摘　　要：介绍了一种含环氧基聚酯的羟值测定方法,即乙酰氯法。通过对其酰化原理分析,选用乙酰氯作酰化剂、二氯甲烷作酰化溶剂,测定含环氧基聚酯的羟值。结果发现无抱团现象,测定结果误差较小。A method for determining hydroxyl value of epoxy-containing polyester, namely acetyl chloride method is introduced. The hydroxyl value of epoxy-containing polyester was determined by analyzing aeetification principle and using aeetyl chloride as acetifier and methylene chloride as solvent.The results Show that there is not coagulation in experiments,and the deviation is small.

关 键 词：乙酰氯法 环氧基 聚酯 羟值 

分 类 号：TQ430.1[化学工程]