用软件定标技术扩展EM－360L核磁共振谱仪的温度适应范围  

To Expand the Operational Temperature Scope of EM-360L NMR by Means of Software Calibration

作　　者：费振义[1] 刘炬民[1] 尚蕾 郭晓燕 

机构地区：[1]山东工业大学测试中心

出　　处：《分析测试技术与仪器》1996年第4期38-41,共4页Analysis and Testing Technology and Instruments

摘　　要：利用计算机控制和数据处理技术对进口核磁共振谱仪加以改造，使其测试所要求的环境温度由原来的恒温（２０±１℃）降至室温。其精度保持不变，硬件方案简捷可靠、软件利用一个标准样品的已知参数来校正系统的刻度单位，算法采用动态的可调刻度单位标定其它样品的测试结果，取得了较为理想的效果。An imported NMR spectrometer is modified by applying computer control and data-processing technique. The operational temperature is changed from 20±1℃ to room temperature while its precision keeps unchanged. The hardware scheme is simple and reliable. Using known parameters of a standard sample, the software corrects the graduation unit of the system. Dynamic adjustable graduation unit is adopted for the algorithm. Known parametres of a standard sample are approached through double-identification and multi-repetition. The test results of other samples by using corrected graduation unit are satisfactory. Factors and regularities affecting the precision of the NMR spectrometer are also discussed.

关 键 词：化学位移 磁场扫描 环境温度 定标 NMR 

分 类 号：O657.99[理学—分析化学]